HRID1760487

反应详情

EQUATION

反应方程式

HRID 1760487 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 4-chloromethyl-5-methyl-2-phenylimidazole.HCl (40.5 g) in dimethylsulfoxide (400 ml) was added to a stirred solution of sodium cyanide (80 g) in dimethylsulfoxide (600 ml) over a period of 30 min. After 20 h the solids were filtered off, washed with water and dried in vacuo.

WORKUP

后处理

  1. filtrationAfter 20 h the solids were filtered off
  2. washwashed with water
  3. customdried in vacuo