Potassium Carbonate → HCID 19858315, compound

HRID 1762129Notes

Reaction equation

HRID 1762129 reaction equation
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

Product 1

HCID 19858315HCID 19858315, compound

Reagents, catalysts & solvents 1

HCID 24813Phosphorus oxychlorideCatalyst

Procedure

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and was concentrated to obtain the product as an oil.

Workup

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationwas concentrated

Sources & evidence

ORD record
ord-42518c203af64540aaafefcd08cba9c2
Source dataset
uspto-grants-1989_05
Patent number
US04831035

Reaction notes

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