HRID1762357

反应详情

EQUATION

反应方程式

HRID 1762357 的结构方程式

PROCEDURE

实验过程

A solution of 19.9 g (0.1 mol) of 1-benzylideneamino-2-ethyl-imidazole in 200 ml of 1.5N hydrochloric acid is subjected to a steam distillation until benzaldehyde no longer results. The mixture is evaporated and the product obtained is recrystallized from ethanol/ether. There are obtained 14.5 g of 1-amino-2-ethylimidazole hydrochloride of melting point 90°-91°.

WORKUP

后处理

  1. customno longer results
  2. customThe mixture is evaporated
  3. customthe product obtained
  4. customis recrystallized from ethanol/ether