HRID1763740

反应详情

EQUATION

反应方程式

HRID 1763740 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 148 g. of 5-p-methoxybenzyl hydantoin and 188 g. of sodium hydroxide in one liter of water is heated at reflux for 25 hours. The solution is cooled and made acid to pH 1 with concentrated hydrochloric acid. The formed solid is separated by filtration, washed with water and dried to give the above named compound, mp. 255° C. dec.

WORKUP

后处理

  1. temperatureat reflux for 25 hours
  2. temperatureThe solution is cooled
  3. customThe formed solid is separated by filtration
  4. washwashed with water
  5. customdried
  6. customto give the