HRID1766671

反应详情

EQUATION

反应方程式

HRID 1766671 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 4-(4-benzyloxy-3-iodophenoxy)-5-methyl-7-nitroindane (4.18 g) in ethyl acetate (15 mL) was added 5% Pt/C (860 mg). The mixture was stirred under a hydrogen atmosphere at room temperature for 2 hours. The insoluble material was removed by filtration. The filtrate was evaporated under reduced pressure to dryness to give the title compound (3.89 g).

WORKUP

后处理

  1. customThe insoluble material was removed by filtration
  2. customThe filtrate was evaporated under reduced pressure to dryness