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HRID1767937

反应详情

EQUATION

反应方程式

HRID 1767937 的结构方程式

REACTANTS

反应物

4
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：CC(C)(C)OC(=O)N=NC(=O)OC(C)(C)C
HCID97268

Di-tert-butyl azodicarboxylate

C10H18N2O4

结构：Cc1c[nH]c2cc(O)ccc12
HCID13662595

6-Hydroxyskatole

C9H9NO

结构：Cc1nc(-c2ccc(C(F)(F)F)cc2)sc1CCO
HCID22647583

2-{4-Methyl-2-[4-(trifluoromethyl)phenyl]-1,3-thiazol-5-yl}ethan-1-ol

C13H12F3NOS

PRODUCTS

生成物

1
结构：Cc1nc(-c2ccc(C(F)(F)F)cc2)sc1CCOc1ccc2c(C)c[nH]c2c1
HCID23614495

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 3 c], 3-methyl-1H-indol-6-ol was reacted with 2-[4-methyl-2-(4-trifluoromethyl-phenyl)-thiazol-5-yl]-ethanol (example 5 c]) in the presence of triphenylphosphine and di-tert-butyl azodicarboxylate to yield 3-methyl-6-{2-[4-methyl-2-(4-trifluoromethyl-phenyl)-thiazol-5-yl]-ethoxy}-1H-indole as yellow solid.