反应详情

温度

0 °C

A reaction vessel was charged with 5.7 g of p-terphenyl and 40 ml of methylene chloride. To this mixture was added 4 g of anhydrous aluminum chloride with stirring at 0° C. A solution of 5.2 g of decanoyl chloride in 10 ml of methylene chloride was added dropwise. After the dropwise addition, the mixture was stirred for 5 hours. The reaction liquid was poured into diluted hydrochloric acid and the mixture was stirred well. Insolubles were collected by filtration, washed and dried to obtain 6.8 g (71%) of 4-decanoyl-p-terphenyl.

1. additionAfter the dropwise addition
2. stirringthe mixture was stirred for 5 hours
3. customThe reaction liquid
4. stirringthe mixture was stirred well
5. filtrationInsolubles were collected by filtration
6. washwashed
7. customdried