反应详情

In the same apparatus and procedures as EXAMPLE 1, 6.0 g (0.027 mole) of 3-phenyl-1,1-dichloro-1-silabutane, 4.1 g (0.05 mole) of cyclohexene, and 90 μl of 1% chloroplatinic acid in isopropanol were placed under the dry nitrogen atmosphere. The reactor was sealed and the solution was stirred for 3 hours. Vacuum distillation of the reaction products gave 7.4 g (bp, 157°-9° C./0.05 mmHg) of 1-cyclohexyl-1,1-dichloro-3-phenyl-1-silabutane.

1. customThe reactor was sealed
2. distillationVacuum distillation of the reaction products