Toluene → Monolaurin

HRID 1770357Notes

Reaction equation

HRID 1770357 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][CH:16]([OH:19])[CH2:17][OH:18])=[O:13].C1(C)C=CC=CC=1.C(C(C)=[O:30])C>C(O)(C)C>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][CH:16]([OH:19])[CH2:17][OH:18])=[O:13].[C:12]([OH:14])(=[O:13])[C:11]1[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=1)[OH:30]

Participants

6

Reactant 3

HCID 1140TolueneHCID 6569Methyl Ethyl KetoneHCID 14871Monolaurin

Product 2

HCID 338Salicylic AcidYield 10%HCID 14871MonolaurinYield 20%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

A fluid solution of 20.0% Lauricidin, 10.0% salicylic acid, and 10.0% DOSS surfactant in isopropanol was prepared by stirring the mixture until the Lauricidin was dissolved. 20% of the fluid solution was combined with 80% of the hardcoat mixture described in Examples 1-11 (i.e., 100 parts of 3M 906 Hardcoat with 12 parts toluene and 12 parts methyl ethyl ketone). The combined solution was coated and cured as described in Examples 1-11. The resulting multi-layer film was clear and transparent. The resulting multi-layer film was then tested for microbial load reduction, as described above in Examples 1-11, and gave 100% microbial load reduction for gram positive pathogens and 99.4% microbial load reduction for gram negative pathogens.

Workup

  1. dissolutionwas dissolved
  2. customgave 100% microbial load reduction for gram positive pathogens and 99.4% microbial load reduction for gram negative pathogens

Sources & evidence

ORD record
ord-628b2d626b2d4d7b8566dd0f610afc84
Source dataset
uspto-grants-2016_02
Patent number
US09247736B2

Reaction notes

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