Hydrochloric Acid → HCID 178508028, compound

HRID 1780002Notes

Reaction equation

HRID 1780002 reaction equation
C(O[N:6]1[C@H:15]2[C@H:10]([CH2:11][CH2:12][CH2:13][CH2:14]2)[NH:9][C:8](=[NH:16])[CH2:7]1)(C)(C)C.Cl>CCOC(C)=O>[NH:16]=[C:8]1[CH2:7][NH:6][C@H:15]2[C@H:10]([CH2:11][CH2:12][CH2:13][CH2:14]2)[NH:9]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 178454423HCID 178454423, compound

Product 1

HCID 178508028HCID 178508028, compoundYield 102.3%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

To 46 mg of 4-t-butoxy-2-imino-decahydro-cis-quinoxaline 3 mL of EtOAc saturated with HCl was added. The reaction turned clear momentarily and another solid was formed. After 30 min the solid was filtered washed with Et2O and dried to furnish 32 mg of the title compound.

Workup

  1. customanother solid was formed
  2. filtrationAfter 30 min the solid was filtered
  3. washwashed with Et2O
  4. customdried

Sources & evidence

ORD record
ord-1fda862840e64c68aab9559135356a1e
Source dataset
uspto-grants-1997_05
Patent number
US05629322

Reaction notes

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