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HRID1784727

反应详情

EQUATION

反应方程式

HRID 1784727 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc([N+](=O)[O-])cn1
HCID77888

2-Pyridinamine, 5-nitro-

C5H5N3O2

结构：CC(Br)C=O
HCID350624

2-bromopropanal

C3H5BrO

PRODUCTS

生成物

1
结构：Cc1cnc2ccc([N+](=O)[O-])cn12
HCID21827346

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Operations similar to Production Example 1-(2) were conducted using 2-bromopropionaldehyde and 2-amino-5-nitropyridine. The solid whereupon obtained was suspended in ethyl acetate, and washed with saturated aqueous sodium hydrogencarbonate solution to provide the title compound as yellow solid.

WORKUP

后处理

  1. customThe solid whereupon obtained
  2. washwashed with saturated aqueous sodium hydrogencarbonate solution