反应详情

A solution of [2-(3-Cyano-phenyl) -1-methyl-ethyl]-carbamic acid tert-butyl ester (180 mg, 0.69 mmol) in dichloromethane (5 mL) and trifluoroacetic acid (5 mL) was stirred for 15 min at room temperature. Solvents removed under vacuum, and residue was partitioned between dichloromethane and 1 N sodium hydroxide. Organic dried over magnesium sulfate and reduced to an oil under vacuum. M+1=161.

1. customSolvents removed under vacuum, and residue
2. customwas partitioned between dichloromethane and 1 N sodium hydroxide
3. dry with materialOrganic dried over magnesium sulfate