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HRID1787989

反应详情

EQUATION

反应方程式

HRID 1787989 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(=O)Nc1ccc(S(=O)(=O)NC(C)(C)C)cc1
HCID668309

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NS(=O)(=O)c1ccc(N)cc1
HCID832627

4-amino-N-tert-butylbenzenesulfonamide

C10H16N2O2S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Na+].[OH-]
溶剂HCID14798

Sodium Hydroxide

HNaO

PROCEDURE

实验过程

N-(1,1-Dimethylethyl)-4-(acetylamino)benzenesulfonamide (Example 11) is deprotected by saponification in 20% NaOH (5 mL), followed by neutralization with 10% HCl. The precipitate that is formed is collected by filtration and recrystallized from methanol/diethyl ether.

WORKUP

后处理

  1. customThe precipitate that is formed
  2. filtrationis collected by filtration
  3. customrecrystallized from methanol/diethyl ether