2-Bromoethyl ethyl ether → HCID 5276125, compound

HRID 1788442Notes

Reaction equation

HRID 1788442 reaction equation
[Cl:1][C:2]1[CH:46]=[CH:45][C:5]([C:6]2[C:11]([C:12]3[CH:21]=[CH:20][C:19]4[C:14](=[CH:15][CH:16]=[C:17]([C:22]5[N:26]([CH:27]6[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]6)[C:25]6[CH:33]=[CH:34][C:35]([C:37]([OH:39])=[O:38])=[CH:36][C:24]=6[N:23]=5)[CH:18]=4)[N:13]=3)=[CH:10][C:9]([O:40][CH2:41][CH2:42][O:43][CH3:44])=[CH:8][CH:7]=2)=[CH:4][CH:3]=1.Br[CH2:48]COCC.BrCCOC>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]2[C:11]([C:12]3[CH:21]=[CH:20][C:19]4[C:14](=[CH:15][CH:16]=[C:17]([C:22]5[N:26]([CH:27]6[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]6)[C:25]6[CH:33]=[CH:34][C:35]([C:37]([OH:39])=[O:38])=[CH:36][C:24]=6[N:23]=5)[CH:18]=4)[N:13]=3)=[CH:10][C:9]([O:40][CH2:41][CH2:42][O:43][CH2:44][CH3:48])=[CH:8][CH:7]=2)=[CH:45][CH:46]=1

Participants

4

Reactant 3

HCID 611412-Bromoethyl ethyl etherHCID 809722-Bromoethyl methyl etherHCID 5276094HCID 5276094, compound

Product 1

HCID 5276125HCID 5276125, compound

Procedure

The title compound was synthesized as described for Compound 475, except 1-bromo-2-ethoxy ethane was used for alkylation instead of 1-bromo-2-methoxy ethane.

Sources & evidence

ORD record
ord-929375494e55402ca20484b819b4d3e3
Source dataset
uspto-grants-2009_03
Patent number
US07511145B2

Reaction notes

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