HRID1789801

反应详情

EQUATION

反应方程式

HRID 1789801 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Acetylsulfanylmethyl-3-(2-amino-pyridin4-yl)-propionic acid ethyl ester (52 mg, 0.13 mmol) was dissolved in conc. HCl (2 mL) under argon. The solution was heated to reflux for 1 h. Concentration under reduced pressure gave the title compound as the hydrochloride salt (32 mg, 100%).

WORKUP

后处理

  1. temperatureThe solution was heated
  2. temperatureto reflux for 1 h
  3. concentrationConcentration under reduced pressure