HRID1789915

反应详情

EQUATION

反应方程式

HRID 1789915 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl )-3-phenyl-propionic acid ethyl ester (58 mg, 0.125 mmol) was dissolved in conc. HCl (3.0 mL). The solution was heated to reflux for 130 min under argon. Concentration under reduced pressure gave the title compound as the hydrochloride salt (41 mg, 100%).

WORKUP

后处理

  1. temperatureThe solution was heated
  2. temperatureto reflux for 130 min under argon
  3. concentrationConcentration under reduced pressure