反应详情

A mixture of DL-glycerinaldehyde (4,5 g, 50 mmole) and (benzyloxycarbonylmethyl)-triphenyl-phosphoniumbromide (24.57 g, 50 mmole) in 100 ml 1,2-epoxybutane was refluxed overnight. The mixture was evaporated under vacuum and the product was isolated by silica gel column chromatography.

1. temperaturewas refluxed overnight
2. customThe mixture was evaporated under vacuum
3. customthe product was isolated by silica gel column chromatography