Azobisisobutyronitrile → HCID 86595652, compound

HRID 1793275Notes

Reaction equation

HRID 1793275 reaction equation
[CH3:1][N:2]([CH3:7])[C:3](=[O:6])[CH:4]=[CH2:5].[CH:8]([CH:10]=[CH2:11])=[O:9].N(C(C)(C)C#N)=NC(C)(C)C#N>O1CCCC1>[CH3:1][N:2]([CH3:7])[C:3](=[O:6])[CH:4]=[CH2:5].[CH:8]([CH:10]=[CH2:11])=[O:9]

Participants

5

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 7847AcroleinHCID 17587N,N-Dimethylacrylamide

Product 1

HCID 86595652HCID 86595652, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

To tetrahydrofuran (300 g) were added N,N-dimethylacrylamide (70 g), acrolein (30 g) and AIBN (2,2′-azobisisobutyronitrile) (5 g). The resulting mixture was reacted at 66° C. for 8 hours. After reaction, the resulting mixture was precipitated in ether, filtered, and dehydrated, thereby obtaining poly(N,N-dimethylacrylamide/acrolein) (45 g).

Workup

  1. customThe resulting mixture was reacted at 66° C. for 8 hours
  2. customAfter reaction
  3. customthe resulting mixture was precipitated in ether
  4. filtrationfiltered

Sources & evidence

ORD record
ord-e406312d98c049aa96999117a8c91f3e
Source dataset
uspto-grants-2006_07
Patent number
US07081325B2

Reaction notes

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