2-Methylindole → HCID 10159534, compound

HRID 1794193Notes

Reaction equation

[CH3:1][C:2]1[NH:3][C:4]2[C:9]([CH:10]=1)=[CH:8][CH:7]=[CH:6][CH:5]=2.[C:11]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:16]=[CH:15][C:14]([CH:17]=O)=[CH:13][CH:12]=1>>[CH3:1][C:2]1[NH:3][C:4]2[C:9]([C:10]=1[CH:17]([C:10]1[C:9]3[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=3)[NH:3][C:2]=1[CH3:1])[C:14]1[CH:15]=[CH:16][C:11]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)=[CH:12][CH:13]=1)=[CH:8][CH:7]=[CH:6][CH:5]=2

Participants

Reactant 2

HCID 72242-Methylindole

HCID 76689(1,1'-Biphenyl)-4-carboxaldehyde

Product 1

HCID 10159534HCID 10159534, compound

Procedure

The compound Bis(2-methylindol-3-yl)-(1,1′-biphenyl-4-yl)methane was prepared following procedure A, starting from 2-methyl indole and 4-biphenyl carboxaldehyde. LC: Tr 2.71 min, MS: 427 (M+H)+

Workup

customTr 2.71 min, MS

Sources & evidence

ORD record: ord-7842f31d19194c28ab83d55d3df4c99a
Source dataset: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07022730B2

Reaction notes

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