7791-20-0 → HCID 131725688, compound

HRID 1794982Notes

Reaction equation

HRID 1794982 reaction equation
O.O.O.O.O.O.[Cl-:7].[Cl-:8].[Ni+2:9].[CH:10]1[CH:15]=[C:14]([S:16]([O-:19])(=[O:18])=[O:17])[CH:13]=[C:12]([P:20]([C:31]2[CH:36]=[CH:35][CH:34]=[C:33]([S:37]([O-:40])(=[O:39])=[O:38])[CH:32]=2)[C:21]2[CH:26]=[CH:25][CH:24]=[C:23]([S:27]([O-:30])(=[O:29])=[O:28])[CH:22]=2)[CH:11]=1.[Na+:41].[Na+].[Na+]>O>[Cl:7][Ni:9][Cl:8].[CH:35]1[CH:34]=[C:33]([S:37]([O-:40])(=[O:39])=[O:38])[CH:32]=[C:31]([P:20]([C:12]2[CH:11]=[CH:10][CH:15]=[C:14]([S:16]([O-:19])(=[O:17])=[O:18])[CH:13]=2)[C:21]2[CH:26]=[CH:25][CH:24]=[C:23]([S:27]([O-:30])(=[O:29])=[O:28])[CH:22]=2)[CH:36]=1.[Na+:41].[Na+:41].[Na+:41]

Participants

4

Reactant 2

HCID 246457791-20-0HCID 6099338Trisodium 3,3',3''-phosphinetriyltris(benzene-1-sulphonate)

Product 1

HCID 131725688HCID 131725688, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Nickel chloridehexahydrate (0.05 mols) was reacted with tppts (0.12 mols) in water sufficient to dissolve and formed complex was precipitated by ethanol

Workup

  1. dissolutionto dissolve
  2. customformed complex
  3. customwas precipitated by ethanol

Sources & evidence

ORD record
ord-87336a187497496c9833f31bcbc48a93
Source dataset
uspto-grants-2006_04
Patent number
US07026266B2

Reaction notes

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