Piperidine → HCID 9902768, compound

HRID 1796930Notes

Reaction equation

HRID 1796930 reaction equation
[N:1]1([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[NH2:12])[CH:5]=[CH:4][CH:3]=[CH:2]1.[Cl-].[CH3:14][C:15]1[CH:16]=[C:17]([CH:25]=[CH:26][CH:27]=1)[CH:18]=[N+:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1.CC1C=C(C=CC=1)C=O.N1CCCCC1>>[N:19]1([CH:18]([C:17]2[CH:16]=[C:15]([CH3:14])[CH:27]=[CH:26][CH:25]=2)[C:5]2[N:1]([C:6]3[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=3[NH2:12])[CH:2]=[CH:3][CH:4]=2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

5

Reactant 4

HCID 8082PiperidineHCID 121053-MethylbenzaldehydeHCID 801232-(1H-pyrrol-1-yl)anilineHCID 17912319HCID 17912319, compound

Product 1

HCID 9902768HCID 9902768, compound

Procedure

The preparation was carried out in accordance with general synthesis instructions 4 from 2-pyrrol-1-yl-phenylamine and 1-(3-methyl-benzylidene)-piperidinium chloride, which had been prepared in accordance with example 3 from 3-methylbenzaldehyde and piperidine.

Sources & evidence

ORD record
ord-3c55e722fd5047e2aa6d42eb294bf593
Source dataset
uspto-grants-2006_04
Patent number
US07034018B2

Reaction notes

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