Itaconic acid → 1-Octyl-5-oxopyrrolidine-3-carboxylic acid

HRID 1801405Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:10]([OH:18])(=[O:17])[C:11]([CH2:13][C:14](O)=[O:15])=[CH2:12].N(CCO)(CCO)CCO>>[CH2:1]([N:9]1[C:14](=[O:15])[CH2:13][CH:11]([C:10]([OH:18])=[O:17])[CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 3

HCID 811Itaconic acid

HCID 7618Triethanolamine

HCID 8143Octylamine

Product 1

HCID 940891-Octyl-5-oxopyrrolidine-3-carboxylic acidYield 162.3%

Procedure

129 g of octylamine, 130 g of itaconic acid and 149 g of triethanolamine were used to obtain 391 g of N-octyl-5-oxopyrrolidine-3-carboxylic acid triethanolammonium salt with

Sources & evidence

ORD record: ord-49add6e8b34b46419552963b7cef9e0a
Source dataset: uspto-grants-2013_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08349215B2

Reaction notes

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