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HRID1804024

反应详情

EQUATION

反应方程式

HRID 1804024 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc(I)cc1
HCID74373

Benzoyl chloride, 4-iodo-

C7H4ClIO

结构：Cc1cnc(N2CCNCC2)c(C)c1
HCID58484496

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(N2CCN(C(=O)c3ccc(I)cc3)CC2)c(C)c1
HCID58484535

未命名化合物

收率 95.6%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 8 and using 1-(3,5-dimethylpyridin-2-yl)piperazine (3.8 g) described in Preparation Example 47 and 4-iodobenzoyl chloride (5.3 g), the title compound (8 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 8