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HRID1804044

反应详情

EQUATION

反应方程式

HRID 1804044 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc(I)cc1
HCID74373

Benzoyl chloride, 4-iodo-

C7H4ClIO

结构：Cc1cc(C2CC2)cnc1N1CCNCC1
HCID58484718

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C2CC2)cnc1N1CCN(C(=O)c2ccc(I)cc2)CC1
HCID58484841

未命名化合物

收率 90%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 65 and using 1-(5-cyclopropyl-3-methylpyridin-2-yl)piperazine (1.42 g) described in Preparation Example 96, 4-iodobenzoyl chloride (1.83 g), the title compound (2.63 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 65