HRID1804107

反应详情

EQUATION

反应方程式

HRID 1804107 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 88 and using 1-Boc-piperazine (2.0 g) and 3-bromo-2,6-dimethylpyridine (2.0 g), a compound was obtained. To the compound were added water and potassium carbonate, and the mixture was extracted with ethyl acetate. The solvent was evaporated to give the title compound (2.01 g).

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 88
  3. customa compound was obtained
  4. extractionthe mixture was extracted with ethyl acetate
  5. customThe solvent was evaporated