HRID1818045

反应详情

EQUATION

反应方程式

HRID 1818045 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The compound was prepared as described in Example 37 by adding piperidine to a solution of 4-hydroxy-3-methoxycinnamaldehyde (35 mg, 0.2 mmol) and N-(cyanoacetyl)benzylamide (34 mg, 0.2 mmol) in ethanol. After recrystallization from ethanol-water a yellow solid was obtained (50 mg, 75%). The product gave the following analytical data:

WORKUP

后处理

  1. customThe compound was prepared
  2. customAfter recrystallization from ethanol-water a yellow solid
  3. customwas obtained (50 mg, 75%)
  4. customThe product gave the following analytical data