反应详情

4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).

1. temperatureheated
2. temperatureat reflux for 3 hours
3. filtrationfiltered
4. washthe residue washed with ether (50 mL)
5. customThe combined filtrate and washings were evaporated