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HRID1828041

反应详情

EQUATION

反应方程式

HRID 1828041 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)NCCc1ccccn1
HCID22027815

tert-Butyl [2-(pyridin-2-yl)ethyl]carbamate

C12H18N2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCC1CCCCN1
HCID5001226

2-(Boc-2-aminoethyl)piperidine

C12H24N2O2

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[O]=[Pt]=[O]
催化剂HCID345198

Platinic oxide

O2Pt

结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

The product from step A was mixed with PtO2 (640 mg) in HOAc (30 mL) and hydrogenation was carried out at 58 psi on a Parr apparatus for overnight. Catalyst was removed and solvent was evaporated under reduced pressure to give N-t-butoxycarbonyl 2-(piperidin-2-yl) ethylamine as a black liquid.

WORKUP

后处理

  1. customCatalyst was removed
  2. customsolvent was evaporated under reduced pressure