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HRID1829727

反应详情

EQUATION

反应方程式

HRID 1829727 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccc(C)c(C(C)Cl)c1
HCID93700

2-(1-Chloroethyl)-1,4-dimethylbenzene

C10H13Cl

结构：[Na]
HCID5360545

Sodium

Na

结构：[O-][n+]1ccccc1S
HCID178526253

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C)c(C(C)Sc2cccc[n+]2[O-])c1
HCID501135

2-(1-[2,5-dimethylphenyl]-ethylthio)pyridine N-oxide

C15H17NOS

收率 83%

PROCEDURE

实验过程

The intermediate 2-(1-[2,5-dimethylphenyl]-ethylthio)pyridine N-oxide is prepared from 1-(2,5-dimethylphenyl)ethyl chloride and 2-mercaptopyridine N-oxide, sodium salt by the procedure described in U.S. Pat. No. 3,960,542, Example 2. Melting point 118°–120° C. Structure confirmed by IR and NMR.