1-Phenyl-1-propanol → beta-Methylstyrene

HRID 1829954Notes

Reaction equation

HRID 1829954 reaction equation
[C:1]1([CH:7](O)[CH2:8][CH3:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C1(C)C=CC=CC=1>[CH3:9][CH:8]=[CH:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 1

HCID 71471-Phenyl-1-propanol

Product 1

HCID 12500beta-MethylstyreneYield 93.6%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The filtered catalyst above was added to 1-phenyl-1-propanol (0.16 g) in toluene (1 ml). The same procedure as above was followed to afford β-methyl styrene as a colourless oil (0.13 g, 92%).

Sources & evidence

ORD record
ord-98365b8f598a4d2ba2aecc7431e57ce5
Source dataset
uspto-grants-2006_06
Patent number
US07064226B2

Reaction notes

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