Resorcinol → HCID 21388122, compound

HRID 1833948Notes

Reaction equation

HRID 1833948 reaction equation
[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)O.[C:9]1([NH2:19])[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11][CH:10]=1.P(OC1C=CC=CC=1)(OC1C=CC=CC=1)OC1C=CC=CC=1>>[OH:5][C:4]1[CH:3]=[C:1]([CH:8]=[CH:7][CH:6]=1)[NH:19][C:9]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 3

HCID 5054ResorcinolHCID 7540Triphenyl phosphiteHCID 86401-Naphthylamine

Product 1

HCID 21388122HCID 21388122, compoundYield 86%

Procedure

Using the method described in Example 1, 220 parts of resorcinol, 286 parts of α-naphthylamine and 8 parts of triphenyl phosphite give 411 parts (86% of theory) of 3-hydroxy-N-naphthyl-aniline, of boiling point 225° - 227° C/2 mm Hg.

Sources & evidence

ORD record
ord-d213964dbb034b06adf8e16f4609c8d4
Source dataset
uspto-grants-1978_01
Patent number
US04067903

Reaction notes

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