Isopropanol → HCID 85937510, compound

HRID 1834011Notes

Reaction equation

HRID 1834011 reaction equation
[O:1]([C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CC(O)C.[CH3:18][S:19]([OH:22])(=[O:21])=[O:20]>CCOCC>[CH3:18][S:19]([OH:22])(=[O:21])=[O:20].[O:1]([C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 3776IsopropanolHCID 6395Methanesulfonic AcidHCID 2005103-Phenoxypyridine

Product 1

HCID 85937510HCID 85937510, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of 18 g. of 3-phenoxypyridine in 100 ml. of 2-propanol is treated with 9.6g. of methanesulfonic acid with stirring. The solution is diluted with ether and the crystalline precipitate of 3-phenoxypyridine methanesulfonate is collected, washed with ether and dried at reduced pressure; m.p. 121°-123° C.

Workup

  1. customthe crystalline precipitate of 3-phenoxypyridine methanesulfonate is collected
  2. washwashed with ether
  3. customdried at reduced pressure

Sources & evidence

ORD record
ord-7bd85d8281e543439c81879c6b041e86
Source dataset
uspto-grants-1978_01
Patent number
US04067983

Reaction notes

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