Phenacyl bromide → HCID 22748664, compound

HRID 1834770Notes

Reaction equation

HRID 1834770 reaction equation
[CH2:1]([N:17]([CH3:19])[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:20]([Br:29])[C:21]([C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)=[O:22]>C(O)C>[Br-:29].[CH2:1]([N+:17]([CH2:20][C:21]([C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)=[O:22])([CH3:19])[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 6259Phenacyl bromideHCID 16221Dimethylhexadecylamine

Product 1

HCID 22748664HCID 22748664, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of hexadecyldimethylamine (0.1 mol) and phenacyl bromide (0.1 mol) in ethanol was refluxed for 5 hours. Ethanol was removed under reduced pressure and the product was crystallised from acetone.

Workup

  1. temperaturewas refluxed for 5 hours
  2. customEthanol was removed under reduced pressure
  3. customthe product was crystallised from acetone

Sources & evidence

ORD record
ord-c41bb479f1994e98a03105fb0caccfb1
Source dataset
uspto-grants-1978_01
Patent number
US04071523

Reaction notes

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