Benzyl Chloride → 2,3-Diphenylpropiononitrile

HRID 1834898노트

반응식

HRID 1834898 반응식
[C:1]1([CH:7]([C:15]2NCCN[N:16]=2)[CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(C#N)C1C=CC=CC=1.C(Cl)C1C=CC=CC=1>>[C:1]1([CH:7]([CH2:8][C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:15]#[N:16])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

4

반응물 3

HCID 7503Benzyl ChlorideHCID 8794PhenylacetonitrileHCID 1784202253-(1,2-Diphenylethyl)-1,4,5,6-tetrahydro-1,2,4-triazine

생성물 1

HCID 952962,3-Diphenylpropiononitrile

실험 절차

A process for preparing 3-(1,2-diphenylethyl)-1,4,5,6-tetrahydro-1,2,4-triazine which comprises reacting benzyl cyanide with benzyl chloride to produce 2,3-diphenylpropionitrile and cyclizing the 2,3-diphenylpropionitrile with 2-aminoethylhydrazine in the presence of a catalytic amount of elemental sulfur to give 3-(1,2-diphenylethyl)-1,4,5,6-tetrahydro-1,2,4-triazine.

출처 및 근거

ORD 기록
ord-ba6770a7fde542e29096c13fac8f7800
출처 데이터셋
uspto-grants-1978_01
특허 번호
US04071684

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