4-Toluenesulfonyl chloride → HCID 15420427, compound
Reaction equation
[CH3:1][Si:2]([CH3:7])([CH3:6])[CH2:3][CH2:4]O.[S:8](Cl)([C:11]1[CH:17]=[CH:16][C:14]([CH3:15])=[CH:13][CH:12]=1)(=[O:10])=[O:9]>N1C=CC=CC=1>[CH3:1][Si:2]([CH3:7])([CH3:6])[CH2:3][CH2:4][S:8]([C:11]1[CH:17]=[CH:16][C:14]([CH3:15])=[CH:13][CH:12]=1)(=[O:10])=[O:9]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Ex-36a) As depicted in Scheme 10, 2-Trimethylsilylethanol is treated with tosyl chloride in pyridine to give 2-trimethylsilyl-1-tosylethane.
Sources & evidence
- ORD record
- ord-ddaa4088980e42f0bf521bd862e0972f
- Source dataset
- uspto-grants-2004_08
- Patent number
- US06774126B2
Reaction notes
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