反应详情

3-[3-(3,4-Dimethoxyphenyl)-4,5-dihydroisoxazol-5-yl]propanal (20.0 mg, 0.079 mmol), 1-(diphenylmethyl)piperazine (19.94 mg, 0.079 mmol), molecular sieve(5 beads) and NaBH(OAc)3 (50.2 mg, 0.237 mmol) were reacted in 3 mL of methylene chloride for about 12 hr. With the following processes the same as in Example 1, 28.4 mg (72.0%) of the target compound was obtained.