反应详情

4.0 g of methyl 4-formylcinnamate are dissolved in 40 ml methanol and then 1.6 g hydroxylamine-hydrochloride and 1.9 g sodium acetate are added. The mixture is stirred overnight and then diluted with 300 ml water. The precipitate is filtered by suction, dried in vacuo and crystallized from ethyl acetate/petrolether. This gives 3.56 9 of the title compound. The mass spectrum shows the molecular peak MH+ at 206 Da.

1. filtrationThe precipitate is filtered by suction
2. customdried in vacuo
3. customcrystallized from ethyl acetate/petrolether