反应详情

温度

50 °C

100 mg (0.31 mmol) of 6.1 was placed in 0.5 ml dimethylacetamide and then 60 mg (1.1 mmol) sodium methoxide were added. The reaction mixture was stirred for 1 h at 50° C. The mixture was purified by chromatography (RP-HPLC-MS), the corresponding fractions were freeze-dried.

1. customThe mixture was purified by chromatography (RP-HPLC-MS)
2. customthe corresponding fractions were freeze-dried