Styrene Oxide → HCID 11010298, compound

HRID 1857030Notes

Reaction equation

HRID 1857030 reaction equation
[IH:1].[CH2:2]1[O:10][CH:3]1[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>C(OCC)C>[I:1][CH:3]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[CH2:2][OH:10]

Participants

4

Reactant 2

HCID 7276Styrene OxideHCID 24841Hydrogen iodide

Product 1

HCID 11010298HCID 11010298, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Conditions

Temperature
0 °C

Procedure

A 250 ml round bottom flask was charged with 21 ml HI (55% aqueous solution) and cooled to 0° C. Via an addition funnel, 20 grams of styrene oxide in 80 ml of diethylether were added over a one hour period. Diethylether (45 ml) was added and the water phase was separated. The leftover organic solution was dried with Na2SO4 and evaporated. Thirty-eight grams of a faint yellow solid were obtained having a melting point of 71-72° C.

Workup

  1. customthe water phase was separated
  2. dry with materialThe leftover organic solution was dried with Na2SO4
  3. customevaporated

Sources & evidence

ORD record
ord-89e16d49200d47a9bbe3a9a7475d2ee1
Source dataset
uspto-grants-2000_11
Patent number
US06143848

Reaction notes

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