HRID1857198

反应详情

EQUATION

反应方程式

HRID 1857198 的结构方程式

CONDITIONS

反应条件

温度
170 °C

PROCEDURE

实验过程

A mixture of 4-chloro-6,7-dimethoxyquinoline (112 mg) and commercially available 3-hydroxybenzophenone (297 mg) was stirred at 170° C. for 10 minutes, the reaction mixture was then purified by thin layer chromatography on silica gel eluting with hexane/acetone (2/1) to obtain 126 mg of the title compound (yield: 65%).

WORKUP

后处理

  1. customthe reaction mixture was then purified by thin layer chromatography on silica gel eluting with hexane/acetone (2/1)