1-Propanol → HCID 18625150, compound

HRID 1859370Notes

Reaction equation

HRID 1859370 reaction equation
[C:1]([N:14]([CH2:16][C:17]([OH:19])=[O:18])[CH3:15])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].S(=O)(=O)(O)O.[CH2:25](O)[CH2:26][CH3:27]>>[CH2:25]([O:18][C:17](=[O:19])[CH2:16][N:14]([C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:15])[CH2:26][CH3:27]

Participants

4

Reactant 3

HCID 10311-PropanolHCID 1118Sulfuric AcidHCID 7348Lauroylsarcosine

Product 1

HCID 18625150HCID 18625150, compound

Procedure

Sixty-one(61) grams of N-lauroylsarcosine (ex. Kawaken Fine Chemicals Co., Ltd.) and 200 ml of 1-propanol were charged into a 500-milliliter flask. Further, 1.45 g of conc. sulfuric acid were added as the catalyst. The mixture was heated under reflux for reaction for 7 hours.

Workup

  1. temperatureThe mixture was heated
  2. temperatureunder reflux for reaction for 7 hours

Sources & evidence

ORD record
ord-a15ce7158bf74f9fb95edbe4347f6e1a
Source dataset
uspto-grants-2003_03
Patent number
US06528068B1

Reaction notes

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