Hydrochloric Acid → HCID 56828137, compound

HRID 1859849Notes

Reaction equation

HRID 1859849 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]([OH:13])=[O:12].OCC1(OC[C@@H](O)[C@@H](O)[C@H]1O)O.[ClH:26]>C(O)(=O)C.O=[Pt]=O>[ClH:26].[NH:1]1[CH:10]2[CH:5]([CH2:6][CH2:7][CH2:8][CH2:9]2)[CH2:4][CH2:3][CH:2]1[C:11]([OH:13])=[O:12]

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 7124Quinaldic AcidHCID 441036D-Psicose

Product 1

HCID 56828137HCID 56828137, compound

Reagents, catalysts & solvents 2

HCID 345198Adams' catalystCatalystHCID 176Acetic AcidSolvent

Procedure

A mixture of PtO2 (25 wt. %) and 2-quinolinecarboxylic acid (Aldrich) in acetic acid was hydrogenated at RT under 60 Psi overnight. The reaction mixture was stripped to dryness. Concentrated HCl was added and stripped to dryness to give the title compound as a white solid.

Sources & evidence

ORD record
ord-4131b6b4a1164d4a85e21859c1fd37a4
Source dataset
uspto-grants-2003_03
Patent number
US06528505B1

Reaction notes

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