HRID1862271

反应详情

EQUATION

反应方程式

HRID 1862271 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 5-benzyloxy-4-{1-(methoxycarbonyl)ethoxy}pyrimidine, 10% palladium/carbon and ethyl acetate is stirred for 3 hours at room temperature under hydrogen atmosphere. The reaction system is purged with nitrogen, then, the reaction solution is filtrated through Celite, and the filtrate is concentrated to obtain 5-hydroxy-4-{1-(methoxycarbonyl)ethoxy}pyrimidine.

WORKUP

后处理

  1. customThe reaction system is purged with nitrogen
  2. filtrationthe reaction solution is filtrated through Celite
  3. concentrationthe filtrate is concentrated