Diethylamine → HCID 57153238, compound

HRID 1871005Notes

Reaction equation

HRID 1871005 reaction equation
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].[Br:6][C:7]([CH2:9]Br)=[CH2:8]>>[CH2:1]([N:3]([CH2:4][CH3:5])[CH:8]=[C:7]([Br:6])[CH3:9])[CH3:2]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 105522,3-Dibromopropene

Product 1

HCID 57153238HCID 57153238, compound

Procedure

Compound 6b is preferably synthesized by reacting diethylamine with 2,3-dibromopropene to produce 1-diethylamino-2-bromo-propene. Copper iodide is then added with THF and the mixture is cooled to below about -78° C. The solution is stirred and allowed to gradually rise to room temperature. The mixture may then be opened to air and poured into a solution of saturated ammonium chloride. Compound 6a may then be extracted with, e.g., ether, and dried.

Sources & evidence

ORD record
ord-2c718b986e1f426697818ef52f261404
Source dataset
uspto-grants-2000_08
Patent number
US06100373

Reaction notes

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