HRID1871370

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6358

2-Bromopropane

C3H7Br

结构：COc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID10913208

未命名化合物

结构：COc1ccc(C2=NN(C)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID70003942

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(C2=NN(C(C)C)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID70002414

未命名化合物

PROCEDURE

实验过程

Prepared from compound 1 and 2-bromopropane as described for compound 8. Purified by chromatography (dichloromethane). Crystallized from diethyl ether/petroleum ether (60-95° C.). M.p. 79-81° C.

WORKUP

后处理

customPurified by chromatography (dichloromethane)
customCrystallized from diethyl ether/petroleum ether (60-95° C.)