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HRID1872670

反应详情

EQUATION

反应方程式

HRID 1872670 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：Cc1cc(Br)cc(C)c1OCC1CCCN(C)C1
HCID9948656

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Br)cc(C)c1OCC1CCCN(C)C1.Cl
HCID21184168

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

The 3-(4-bromo-2,6-dimethylphenoxymethyl)-1 -methylpiperidine was treated with 1N hydrochloric acid in ether, and the precipitated salt was recrystallized from acetonitrile/tert-butyl methyl ether to yield 3-(4-bromo-2,6-dimethylphenoxymethyl)-1-methylpiperidine hydrochloride, m.p. 180.9-183.5° C.

WORKUP

后处理

  1. customthe precipitated salt was recrystallized from acetonitrile/tert-butyl methyl ether