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HRID1879005

反应详情

EQUATION

反应方程式

HRID 1879005 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COCCBr
HCID80972

Ethane, 1-bromo-2-methoxy-

C3H7BrO

结构：OC(c1cccc(C2CCNCC2)c1F)C(F)(F)F
HCID57448056

未命名化合物

PRODUCTS

生成物

1
结构：COCCN1CCC(c2cccc(C(O)C(F)(F)F)c2F)CC1
HCID67533216

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Preparation according to Example 1: 2,2,2-trifluoro-1-(2-fluoro-3-piperidin-4-ylphenyl)ethanol (0.01 g), acetonitrile (2 ml), potassium carbonate (0.01 g) and 1-bromo-2-methoxyethane (0.01 g). MS m/z (rel. intensity, 70 eV) 335 (M+, 1), 291 (15), 290 (bp), 207 (4), 149 (7).

WORKUP

后处理

  1. customPreparation