huagongshe.com
HRID1879804

反应详情

EQUATION

反应方程式

HRID 1879804 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)C(=O)O
HCID6417

2,2-Dimethylpropanoic acid

C5H10O2

结构：CN1C(C)(C)CC(=NO)CC1(C)C
HCID241950

N-(1,2,2,6,6-Pentamethylpiperidin-4-ylidene)hydroxylamine

C10H20N2O

结构：CC(=O)[O-].CC(=O)[O-].CC(=O)[O-].CC(=O)[O-].[Pb+4]
HCID178418268

未命名化合物

PRODUCTS

生成物

1
结构：CN1C(C)(C)CC(N=O)(OC(=O)C(C)(C)C)CC1(C)C
HCID57954471

未命名化合物

PROCEDURE

实验过程

1,2,2,6,6-Pentamethyl-4-nitrosopiperidin-4-yl pivalate was prepared from 1,2,2,6,6-pentamethyl-piperidin-4-one oxime, lead tetraacetate and trimethylacetic acid using conditions of General Method 3. 1H NMR (250 MHz, CHLOROFORM-d) δ 2.43-2.64 (5H, m), 2.09 (3H, s), 1.91 (2H, d, 14.2 Hz), 1.39 (6H, d, 5.9 Hz), 1.30 (9H, s), 1.25 (6H, d, 2.6 Hz).