Hydrogen Peroxide → HCID 15746751, compound

HRID 1886222Notes

Reaction equation

[CH2:1]([NH:5][C:6]([NH:8][C:9](=[O:16])[CH2:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])=[O:7])[CH2:2][CH2:3][CH3:4].CS(O)(=O)=[O:19].OO>>[CH2:1]([NH:5][C:6]([NH:8][C:9](=[O:16])[CH2:10][CH2:11][CH2:12][C:13]([O:15][OH:19])=[O:14])=[O:7])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 3

HCID 784Hydrogen Peroxide

HCID 6395Methanesulfonic Acid

HCID 15746750HCID 15746750, compound

Product 1

HCID 15746751HCID 15746751, compound

Procedure

80.8 g (0.35 mol) of N-(N'-butylcarbamoyl)glutaramic acid, 123 g of methanesulfonic acid and 42 g (1.05 mol) of hydrogen peroxide (85% strength by weight) are reacted and worked up as described in Example 3.

Sources & evidence

ORD record: ord-4702673f9b204ef0ac61e52abbbd7099
Source dataset: uspto-grants-1992_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05149864

Reaction notes

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