HRID1890506

反应详情

EQUATION

反应方程式

HRID 1890506 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a mixture of 3-(azidomethyl)-1H-pyrrolo[2,3-b]pyridine (A-4) (1.50 g, 8.63 mmol) in EtOAc (150 mL) was added 10% Pd/C (1.10 g). The resulting reaction mixture was stirred under one atmosphere of H2 at room temperature for 3 h. The mixture was filtered, and the filtrate was concentrated to afford the title compound (1.15 g).

WORKUP

后处理

  1. customThe resulting reaction mixture
  2. filtrationThe mixture was filtered
  3. concentrationthe filtrate was concentrated